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dc.provenanceCONICET-
dc.creatorAridoss, Gopalakrishnan-
dc.creatorZhao, Chunqing-
dc.creatorBorosky, Gabriela Leonor-
dc.creatorLaali, Kenneth K.-
dc.date2018-10-16T20:00:00Z-
dc.date2018-10-16T20:00:00Z-
dc.date2012-04-
dc.date2018-09-18T16:14:51Z-
dc.date.accessioned2019-04-29T15:38:19Z-
dc.date.available2019-04-29T15:38:19Z-
dc.date.issued2012-04-
dc.identifierAridoss, Gopalakrishnan; Zhao, Chunqing; Borosky, Gabriela Leonor; Laali, Kenneth K.; Experimental and GIAO 15N NMR study of substituent effects in 1 H -tetrazoles; American Chemical Society; Journal of Organic Chemistry; 77; 8; 4-2012; 4152-4155-
dc.identifier0022-3263-
dc.identifierhttp://hdl.handle.net/11336/62479-
dc.identifierCONICET Digital-
dc.identifierCONICET-
dc.identifier.urihttp://rodna.bn.gov.ar:8080/jspui/handle/bnmm/298241-
dc.descriptionA series of 1-aryl/alkyl-1H-1,2,3,4-tetrazoles, 5-substituted 1H-tetrazoles, and 1,5- and 2,5-disubstituted 1H-tetrazoles were studied by a combination of experimental NMR (natural abundance 15N, 15N/ 1H HMBC, and 13C) and computational GIAO-NMR techniques to explore substituent effects on 15N (and 13C) NMR chemical shifts in the tetrazole (TA) moiety. Computed 15N chemical shifts via GIAO-B3LYP/6-311+G(2d,p) calculations gave satisfactory results in comparison with experimental data. Whereas N-alkylation leads to large 15N chemical shift changes, changes in the N 1-aryl derivatives bearing diverse substituent(s) are generally small except for polar ortho-substituents (COOH, NO 2). Large δδ 15N values were computed in N 1-aryl derivatives for p-COH 2 + and p-OMeH + as extreme examples of electron-withdrawing substituents on a TA moiety. © 2012 American Chemical Society.-
dc.descriptionFil: Aridoss, Gopalakrishnan. University of North Florida; Estados Unidos-
dc.descriptionFil: Zhao, Chunqing. University of North Florida; Estados Unidos-
dc.descriptionFil: Borosky, Gabriela Leonor. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigaciones en Físico-química de Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Investigaciones en Físico-química de Córdoba; Argentina-
dc.descriptionFil: Laali, Kenneth K.. University of North Florida; Estados Unidos-
dc.formatapplication/pdf-
dc.formatapplication/pdf-
dc.languageeng-
dc.publisherAmerican Chemical Society-
dc.relationinfo:eu-repo/semantics/altIdentifier/doi/https://dx.doi.org/10.1021/jo300242s-
dc.relationinfo:eu-repo/semantics/altIdentifier/url/https://pubs.acs.org/doi/10.1021/jo300242s-
dc.rightsinfo:eu-repo/semantics/restrictedAccess-
dc.rightshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/-
dc.sourcereponame:CONICET Digital (CONICET)-
dc.sourceinstname:Consejo Nacional de Investigaciones Científicas y Técnicas-
dc.sourceinstacron:CONICET-
dc.source.urihttp://hdl.handle.net/11336/62479-
dc.subject15N NMR-
dc.subjectTETRAZOLES-
dc.subjectSUBSTITUENT EFFECTS-
dc.subjectOtras Ciencias Químicas-
dc.subjectCiencias Químicas-
dc.subjectCIENCIAS NATURALES Y EXACTAS-
dc.titleExperimental and GIAO 15N NMR study of substituent effects in 1 H -tetrazoles-
dc.typeinfo:eu-repo/semantics/article-
dc.typeinfo:eu-repo/semantics/publishedVersion-
dc.typeinfo:ar-repo/semantics/articulo-
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